A further increase in depth penetration by
light-interference microscopy can be accomplished with the immersion method.
This consists of observing the specimen surface through a medium with a high
refractive index, such as oil, into which the object, or its replica is being
immersed. With the immersion method, the depth of penetration of
light-interference microscopy can be increased to about 0.001 inch. Figures 15-21
and 15-22 illustrate the advantages of the immersion technique when inspecting
surfaces on which the departures of certain features exceed the discriminating
capacity of regular light-interference microscopes.
Fig. 15-21. (Top)
Interference micrograph of a generally flat surface, interrupted by a deep
groove in the center of the observed area. The abrupt change in level causes the
compression of the fringes beyond the limit of resolution.
Fig. 15-22. (Bottom) The
specimen area shown in Fig. 15-21, as it appears when prepared by immersion
technique. A replica made from the surface is immersed into a medium with high
refractive index, the value of which is considered as a factor when computing
the depth of the now distinctly appearing groove.
While monochromatic light is preferred to obtain a reliable
scale in the form of known fringe separation, most interference microscopes offer
the alternative use of white light, as well, for producing a single dark
fringe, often termed zero fringe. This latter is easier to follow in the
assessment of the interference image when variations of the object surface are
causing fringe shifts that amount to several band widths.
Multiple-beam interference microscopes are sometimes
preferred for the examination of very fine surfaces where the clear definition
of the fringe boundaries offered by the multiple-beam system is required. In
this system, the mutually interfering light beams are forced to pass the
interference space several times, resulting in particularly sharp fringe lines,
permitting measurements in the submicroinch range. The multiple-beam system,
however, requires focusing very close to the objective, which usually limits
its application to flat surfaces of excellent geometry, unless replicas of the
test piece surface are used.
In conclusion, it can be stated that the interference
microscopy, although subjected to certain practical limitations, offers many
technical advantages for the analysis and measurement of surface texture. A few
characteristic properties are mentioned in the following, to permit an
evaluation of the suitability of the interference method for the surface
examination of specific workpieces.
The following are the
limitations
of interference microscopy:
a. The depth range that can be covered by direct
measurements excludes its use for rough surfaces, unless an immersion technique
is applied;
b. It is adaptable only to external surfaces, which are
accessible by the microscope, and of substantially regular form, unless
replicas are made and inspected; and
c. The assessment of surface conditions, as presented by the
interference image, is not directly correlated with the average-roughness
values specified by current standards; however, good correlations exist with
the stylus type, peak-to-valley measurements.
The following are the
advantages
of interference microscopy:
a. It is an area sampling method, which can be visualized
as simultaneously presenting a series of closely spaced cross-sections of the
inspected area;
b. The direction of these imaginary cross-sectional planes,
as well as their spacing, can be selected to provide the most informative
fringe pattern;
c. It offers its own standard of measurement of the highest
accuracy and never requires recalibration;
d. Being a noncontact method, it is nondestructive and
applicable to materials that, because of their softness, could not be inspected
by the stylus method; and
e. Even minute variations of the surface that defeat
faithful scanning with a stylus of finite dimensions can be clearly shown.
Sub-Angstrom, Non-Contact 3D Surface Profiling
Somewhere at the intersection of non-contact electronic
gages, engineering microscopes, contour and form scanning we find a metrology
tool capable surface profiling at the sub-angstrom level (see Fig. 15-23). An
angstrom is one hundred-millionth of a centimeter and given that a nanometer is
one-billionth of a meter, an angstrom is 0.1 (or one-tenth) of a nanometer; the
angstrom is a truly small unit of measure. Coherence correlation interferometry
(CCI) is able to complete a measurement with over one million data points in
less than ten seconds with a resolution of 0.1 angstroms (0.01 nm). Surface
inspection at this level must be accomplished by noncontact means. Surface
quality at nanometer scale is becoming commonplace in optical, semiconductor
and orthopedic component manufacturing. The instrument shown in Fig. 15-23 can
provide critical information related to manufacturing processes working in the
nanometer realm.
Fig. 15-23. “Talysurf CCI” advanced
3-dimensional non-contact metrology tool used for advanced surface
characterization connected to computers and monitors for analysis and graphical
display.
Because the surface features being discussed here are so
small, sophisticated computer software that allows for the analysis and
graphical display of surface images was developed. Taylor Hobson Precision has
its proprietary Talymap software for use with its non-contact 3D surface
profiling products. One company, TrueGage Surface Metrology has developed a
series of software analysis and imaging products that can be used with a
variety of surface measurement products and by their manufacturers. An example
of a topographical “weather map” is shown in Fig. 15-24.
On a computer monitor or in a color copy of the same, the
shades of gray in Fig. 15-24 would be colors of the spectrum making the image
even more vivid and meaningful.
Fig. 15-24. “Truemap”
surface topology visualization and analysis software digital output display.